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液相色谱仪串联质谱的检测流程方法总汇

DIANJICISHU:31 FABUSHIJIAN:2020/1/7 17:53:12

皇冠篮球比分网RUJINDANBAIZU/DAIXIEZUXUEBEIGUANGFANYINGYONGYUSHENGMINGKEXUELINGYU,YEXIANGSEPUYICHUANLIANZHIPUJISHU(YEZHILIANYONG)SHIDANBAIZU/DAIXIEZUXUEYANJIUDEZHUYAOSHOUDUAN,YINCIYEZHILIANYONGSHOUDAOLEYIXUEKEXUEDEJIDAZHONGSHI。NEIMEJINTIANJIULAILEJIEYIXIAYEZHILIANYONGDEJIBENLIUCHENGBA!

 

液相色谱仪

 

液相色谱部分由进样系统、输液系统、分离系统三个部分组成

(1)JINYANGZHUANGZHIYAOQIUMIFENGXINGHAO,SITIJIXIAO,ZHONGFUXINGHAO,BAOZHENGZHONGXINJINYANG,JINYANGSHIDUISEPUXITONGDEYALI、LIULIANGYINGXIANGXIAO。

皇冠篮球比分网(2)SHUYEXITONGZUIWEIZHUYAODESHITIDUXITUOZHUANGZHI——YOULIANGZHONGFANGSHI:YIZHONGCHENGDIYATIDU,ZHICHANGYAXIARONGJIANYIDINGBILIHUNHEHOUZAIYOUGAOYABENGSHURUSEPUZHU,YOUCHENGWAITIDU;LINGYIZHONGCHENGGAOYATIDU,ZHIXIANYONGGAOYABENGJIANGGERONGJISHURUHUNHEQIHUNHE,ZAISONGRUSEPUZHU,YECHENGWEINEITIDU。

(3)FENLIXITONGBAOKUOSEPUZHU、LIANJIEGUANHEHENGWENQIDENG。YUDANCHUNLCXIANGBI,LC-MSYIBANLIUSUJIAODI(GAOLIUSUKENENGYINGXIANGWUHUAXIAOGUO),SUOYIYIBANYONGZHAIJINGZHU,JI2 mmHUO2.1mmDE,LIJINGYIBANWEI3.5μm,YEYOU1.7μmDE。

 

液相色谱仪

 

液相色谱仪分析的一般流程

(1)ESIDIANLI:QIGONGZUOYUANLISHIJIANGYEDIBIANCHENGZHENGQI,CHANSHENGLIZIFASHEDEGUOCHENGZHONGXINGCHENGDERONGJIYOUYEXIANGBENGSHUSONGDAOESI Probe,JINGQINEIDEBUXIUGANGMAOXIGUANLIUCHU,ZHEISHIJIMAOXIGUANJIA2-4 kvDEGAOYA,YOUYUGAOYAHEWUHUAQIDEZUOYONG,LIUDONGXIANGCONGMAOXIGUANDINGDUANLIUCHUSHI,HUIXINGCHENGSHANZHUANGPENWU,SHIYEDISHENGCHENGHANYANGPINHERONGJILIZIDEQIRONGJIAO。ESISHUYUZUIRUANDEDIANLIFANGSHI,TONGCHANGZHICHANSHENGFENZILIZIFENG。SHIHEREBUWENDINGDEJIXINGFENZI,NENGFENXIXIAOFENZIJIDAFENZI。

皇冠篮球比分网(2)SIJIGANZHILIANGFENXIQI:SIJIGANNEISUOBAOWEIDEKONGJIANCUNZAISHUANGQUXIANXINGDIANCHANG。CONGLIZIYUANRUSHEDEJIASULIZICHUANGUOSIJIGANZHONGDEDIANCHANGHUISHOUDAODIANCHANGZUOYONG,ZHIYOUXUANDINGDEm/zLIZIYIXIANDINGDEPINLVWENDINGDETONGGUOSIJIGANZHILIANGFENXIQI,QITALIZIZEPENGDAOJIGANSHANGBEIXILVDIAO,BUNENGTONGGUO,JIDADAO“LVZHI”DEZUOYONG。SIJIGANZHILIANGFENXIQIJIEGOUJINCOU,TIJIXIAO,SAOMIAOSUDUKUAI,SHIYONGYULC-MSLIANYONGYI。

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